By James J. Chopack
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Extra resources for Chemistry Explosives A Multiple Capability Sympathetic Detonator System For The U S Special Forces
The speciﬁc method of preparation is impregnation of the carbonate by a solution containing silver ions and organic complexing agents, such as ethene diamine, oxalic acid, and ethanol amine. The patent discloses the formation of a slurry, which is spread on a ﬂat surface and roasted to remove organic precursors and reduce the silver. The potassium nitrate is added by impregnation after reduction of the silver precursor to the metallic state, but may also be included in the silver precursor solution.
1998, 416, 329. 39. T. A. Nijhuis, B. J. Huizinga, M. Makkee, J. A. Moulijn, Ind. Eng. Chem. Res. 1999, 38, 884. 40. T. Hayashi, K. Tanaka, M. Haruta, Am. Chem. , Div. Pet. Chem. 1996, 41, 71. 41. Y. A. Kalvachev, T. Hayashi, S. Tsubota, M. : R. K. Grasselli, S. T. Oyama, A. M. Gaﬀney, J. E. Lyons, Elsevier Science, 1997, pp. 965–972. 42. E. E. Stangland, K. B. Stavens, R. P. Andres, W. N. Delgass, J. Catal. 2000, 191, 332. 43. H. Orzesek, R. P. Schulz, U. Dingerdissen, W. F. Maier, Chem. Eng. Technol.
In Figs. 14(b), TEM pictures of the Au-TS-1 samples are shown. The morphology of the two samples is quite diﬀerent. TS-1a consisted of very small crystallites (10 nm), agglomerated to form 150 nm particles, whereas TS-1b consisted of 35 µm crystals. The size of the gold particles in the TS-1a sample with the small crystallites, was estimated to be 3–15 nm, which is not signiﬁcantly smaller than those observed on the edges of the large TS-1b crystals. However, titanium is an essential factor in the activity of dispersed gold catalysts in the epoxidation of propene.